声共振混合设备用于百克量级火炸药制备的能量转换特性

(西安近代化学研究所,陕西 西安 710065)

应用化学; 声共振混合; 火炸药; 输入能量; 加速度

Energy Conversion Characteristics of Resonance Acoustic Mixer Used for 100g Level Manufacture of Propellants and Explosives
CHEN Song,MA Ning,XIE Zhong-yuan,QIN Neng,ZHANG Zhe,SUN Xiao-peng,WANG Xiao-feng

(Xi'an Modern Chemistry Research Institute, Xi'an 710065, China)

applied chemistry; resonance acoustic mixing(RAM); propellants and explosives; input energy; acceleration

DOI: 10.14077/j.issn.1007-7812.201907026

备注

为明确声共振混合设备在不同加速度条件下驱动输入能量和混合动能之间的转换特性,掌握声共振混合技术设备放大、工艺放大和工艺控制的基本规律,以200克B炸药、浇注PBX、熔注PBX、HTPE推进剂为混合对象,加速度在0~60g范围内反复改变,测试驱动电机输入能量随加速度变化的关系。结果 表明,声共振混合设备输入能量随着加速度的增大而增大,两者之间呈线性关系,设备反复启停和加速度频繁调节并不会影响这种线性关系,声共振设备具有良好的运行稳定性和重复性; 火炸药混合过程中物料状态的变化、由物料状态变化引起的阻尼变化、由真空度引起的阻尼变化对输入能量和加速度之间的线性关系没有影响; 输入能量和加速度之间的线性关系对被混物料质量的变化较为敏感,相同加速度条件下被混物料质量变大时输入能量也变大; 对于实验所用的混合设备,被混物料为200克时,输入能量和加速度之间线性关系的斜率为0.339,可作为声共振混合设备性能参数标定和工艺控制的依据。

In order to determine the conversion characteristics between input energy of drive motors and the mixing kinetic energy of the resonance acoustic mixer(RAM)under different acceleration conditions, and master the basic rules of equipment amplification, technology amplification and technology control, the relationship between input energy of driving motor and acceleration was tested. Taking Comp.B, cast PBX explosive, melt-cast PBX explosive and HTPE propellant with their mass of 200 gram as mixed objects and the acceleration was changed repeatedly in the range of 0-60g. The results show that there is a linear relationship between the input energy and mixing acceleration, and the input energy increases with the increase of mixing acceleration. The linear relationship is not affected by the repeated start-stop of the equipment and frequent adjustment of acceleration. Therefore, the acoustic resonance equipment has good operation stability and repeatability. In addition, the change of material state in the mixing process, the demping change caused by the change of material state, and the demping change caused by the vacuum have little effect on the linear relationship between input energy and acceleration. However, the linear relationship between the input energy and acceleration is sensitive to the change of the mass of the mixed material, and the input energy increases with the increase of the mass of the mixed material under the same acceleration condition. For the equipment used in this paper, when the mass of mixed material is 200 gram, the slope of the linear relationship is 0.339. This study can provide some guidance for the performance parameter calibration and process control of resonance acoustic mixer.